benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecyl carbamate

Base Information

Chemical Name:benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecyl carbamate
CAS No.:952143-97-4
Molecular Formula:C₃₉H₅₃NO₅
Molecular Weight:615.854
Hs Code.:

Synonyms:benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecyl carbamate

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Chemical Property of benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecyl carbamate

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Technology Process of benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecyl carbamate

There total 6 articles about benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 952143-96-3
benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecen-(3E)-enyl carbamate

: 952143-97-4
benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecyl carbamate

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethyl acetate; at 20 ℃; for 2h; under 3102.97 Torr;
DOI:10.1016/j.tetlet.2007.07.034

Reference yield:

: 865565-60-2
(1R,2S)-1-(p-methoxyphenyl)but-3-ene-1,2-diol

: 952143-97-4
benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecyl carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / NaH / tetrahydrofuran; dimethylformamide / 11 h / 20 °C

2: Na₂CO₃ / toluene / 24 h / -78 °C

3: 11.0 g / Na₂SO₃ / ethyl acetate; H₂O / 24 h / 20 °C

4: 88 percent / Hoveyda 2^nd Grubbs catalyst / toluene / 48 h / 80 °C

5: 70 percent / H₂ / PtO₂ / ethyl acetate / 2 h / 20 °C / 3102.97 Torr

With hydrogen; sodium hydride; sodium carbonate; sodium sulfite; platinum(IV) oxide; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2007.07.034

Reference yield:

: 914618-54-5
(1R,2S)-1,2-bis(benzyloxy)-1-p-methoxyphenylbut-3-ene

: 952143-97-4
benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecyl carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: Na₂CO₃ / toluene / 24 h / -78 °C

2: 11.0 g / Na₂SO₃ / ethyl acetate; H₂O / 24 h / 20 °C

3: 88 percent / Hoveyda 2^nd Grubbs catalyst / toluene / 48 h / 80 °C

4: 70 percent / H₂ / PtO₂ / ethyl acetate / 2 h / 20 °C / 3102.97 Torr

With hydrogen; sodium carbonate; sodium sulfite; platinum(IV) oxide; In water; ethyl acetate; toluene;
DOI:10.1016/j.tetlet.2007.07.034