1-(4-amino-3-iodophenyl)-2,2,2-trifluoroethanone

Base Information

Chemical Name:1-(4-amino-3-iodophenyl)-2,2,2-trifluoroethanone
CAS No.:812640-39-4
Molecular Formula:C₈H₅F₃INO
Molecular Weight:315.034
Hs Code.:

Synonyms:1-(4-amino-3-iodophenyl)-2,2,2-trifluoroethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-amino-3-iodophenyl)-2,2,2-trifluoroethanone

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Technology Process of 1-(4-amino-3-iodophenyl)-2,2,2-trifluoroethanone

There total 4 articles about 1-(4-amino-3-iodophenyl)-2,2,2-trifluoroethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 23516-79-2
4-(trifluoroacetyl)aniline

: 812640-39-4
1-(4-amino-3-iodophenyl)-2,2,2-trifluoroethanone

Guidance literature:: With hydrogenchloride; Iodine monochloride;
DOI:10.1021/ja0294515

Reference yield: 62.0%

: 23516-79-2
4-(trifluoroacetyl)aniline

: 812640-39-4
1-(4-amino-3-iodophenyl)-2,2,2-trifluoroethanone

: 1-(4-amino-3,5-diiodophenyl)-2,2,2-trifluoroethanone

Guidance literature:: With hydrogenchloride; Iodine monochloride; In water; at 20 ℃; for 12h;
DOI:10.1016/j.tet.2004.08.100

Reference yield:

: 655-32-3
2,2,2-trifluoro-1-(4-fluorophenyl)ethanone

: 812640-39-4
1-(4-amino-3-iodophenyl)-2,2,2-trifluoroethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / NH₃ / dimethylsulfoxide

2: 62 percent / ICl; 3N aq. HCl

With hydrogenchloride; ammonia; Iodine monochloride; In dimethyl sulfoxide;
DOI:10.1021/ja0294515