methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

Base Information

Chemical Name:methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside
CAS No.:131291-09-3
Molecular Formula:C₄₁H₄₂N₂O₈SSi
Molecular Weight:750.945
Hs Code.:

Synonyms:methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

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Chemical Property of methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

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Technology Process of methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

There total 1 articles about methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 131291-08-2
methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-β-D-galactopyranoside

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 131291-09-3
methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

Guidance literature:: In toluene; at 100 ℃; for 15h;
DOI:10.1016/0008-6215(90)84033-Q

Reference yield: 95.0%

: 131291-09-3
methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

: 131291-10-6
methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-β-D-xylo-hexopyranoside

Guidance literature:: With tri-n-butyl-tin hydride; In toluene; for 0.75h; Heating;
DOI:10.1016/0008-6215(90)84033-Q

Reference yield:

: 131291-09-3
methyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-O-(imidazol-1-ylthiocarbonyl)-β-D-galactopyranoside

: 131291-11-7
methyl 2,3-di-O-benzoyl-4-deoxy-β-D-xylo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / tributyltin hydride / toluene / 0.75 h / Heating

2: 91 percent / boron trifluoride-methanol / CH₂Cl₂; methanol / 36 h / Ambient temperature

With tri-n-butyl-tin hydride; boron trifluoride methanol complex; In methanol; dichloromethane; toluene;
DOI:10.1016/0008-6215(90)84033-Q