2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-1-O-(p-nitrobenzoyl)-α-L-arabino-hexopyranose

Base Information

Chemical Name:2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-1-O-(p-nitrobenzoyl)-α-L-arabino-hexopyranose
CAS No.:137333-06-3
Molecular Formula:C₁₅H₁₈N₂O₈
Molecular Weight:354.317
Hs Code.:

Synonyms:2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-1-O-(p-nitrobenzoyl)-α-L-arabino-hexopyranose

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Chemical Property of 2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-1-O-(p-nitrobenzoyl)-α-L-arabino-hexopyranose

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Technology Process of 2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-1-O-(p-nitrobenzoyl)-α-L-arabino-hexopyranose

There total 1 articles about 2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-1-O-(p-nitrobenzoyl)-α-L-arabino-hexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65827-72-7,65827-77-2,72398-09-5,72398-10-8,83497-41-0,86427-76-1,98712-70-0
methyl α-L-evernitroside

: 122-04-3
4-nitro-benzoyl chloride

: 137333-06-3
2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-1-O-(p-nitrobenzoyl)-α-L-arabino-hexopyranose

Guidance literature:: With pyridine; sulfuric acid; Yield given. Multistep reaction; 1) aq. dioxane, 90 deg C, 28 h; 2) room temperature, overnight;
DOI:10.1021/jo00025a034

Reference yield: 73.0%

: 116217-59-5
methyl 4-O-(4-benzyloxy-3,5-dichloro-2-methoxy-6-methylbenzoyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

: 137333-06-3
2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-1-O-(p-nitrobenzoyl)-α-L-arabino-hexopyranose

: 137362-89-1
methyl 4-O-(4-benzyloxy-3,5-dichloro-2-methoxy-6-methylbenzoyl)-3-O-(2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-α-L-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -78 ℃; for 0.5h;
DOI:10.1021/jo00025a034

Reference yield: 64.0%

: 18944-96-2
methyl 4-O-benzoyl-2,6-dideoxy-α-D-arabino-hexopyranoside

: 137333-06-3
2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-1-O-(p-nitrobenzoyl)-α-L-arabino-hexopyranose

: 137333-07-4
methyl 4-O-benzoyl-3-O-(2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-α-L-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -78 ℃; for 2h;
DOI:10.1021/jo00025a034