7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine

Base Information

• Chemical Name: 7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine
• CAS No.: 930294-03-4
• Molecular Formula: C₁₆H₁₈ClN₅O₃
• Molecular Weight: 363.804

Synonyms:7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine

Chemical Property of 7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine

Chemical Property:

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Technology Process of 7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine

There total 1 articles about 7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

→ 7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine (930294-03-4)

Guidance literature:

Reference yield: 75.0%

7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine (930294-03-4) + methylamine (74-89-5) → 6-amino-2-(2-methoxyethoxy)-9-(4-((methylamino)methyl)benzyl)-7,9-dihydro-8H-purin-8-one (930294-32-9)

Guidance literature:

7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine; methylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

With ammonia; water; In N,N-dimethyl-formamide;

Reference yield: 55.0%

7,8-Dihydro-9-[4-(chloromethyl)benzyl]-2-(2-methoxyethoxy)-8-oxoadenine (930294-03-4) + methyl {3-[2-(N-methylamino)ethoxy]phenyl}acetate hydrochloride (930778-39-5) → 7,8-dihydro-9-[4-{N-[2-(3-methoxycarbonylmethylphenyl)oxyethyl]-N-methylamino}methylbenzyl]-2-(2-methoxyethoxy)-8-oxoadenine (930784-81-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetone; at 20 - 60 ℃; for 14.5h;

Downstream raw materials:

6-amino-2-(2-methoxyethoxy)-9-(4-((methylamino)methyl)benzyl)-7,9-dihydro-8H-purin-8-one

7,8-dihydro-9-[4-{N-[2-(3-methoxycarbonylmethylphenyl)oxyethyl]-N-methylamino}methylbenzyl]-2-(2-methoxyethoxy)-8-oxoadenine

(3-{2-[9-(4-{[6-Amino-2-(2-methoxyethoxy)-8-oxo-7,8-dihydro-9H-purin-9-yl] methyl}benzyl)-1-oxa-4,9-diazaspiro[5.5]undec-4-yl] ethoxy}phenyl)acetic acid methyl ester

(3-{2-[{[1-(4-{[6-Amino-2-(2-methoxyethoxy)-8-oxo-7,8-dihydro-9H-purin-9-yl] methyl}benzyl)-4-hydroxypiperidin-4-yl]methyl}(methyl)amino]ethoxy}phenyl)acetic acid methyl ester

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