(S)-tert-butyl((5-(2-(pent-4-en-1-yl)-1,3-dioxolan-2-yl)pentan-2-yl)oxy) diphenylsilane

Base Information

Chemical Name:(S)-tert-butyl((5-(2-(pent-4-en-1-yl)-1,3-dioxolan-2-yl)pentan-2-yl)oxy) diphenylsilane
CAS No.:1449688-79-2
Molecular Formula:C₂₉H₄₂O₃Si
Molecular Weight:466.736
Hs Code.:

Synonyms:(S)-tert-butyl((5-(2-(pent-4-en-1-yl)-1,3-dioxolan-2-yl)pentan-2-yl)oxy) diphenylsilane

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Chemical Property of (S)-tert-butyl((5-(2-(pent-4-en-1-yl)-1,3-dioxolan-2-yl)pentan-2-yl)oxy) diphenylsilane

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Technology Process of (S)-tert-butyl((5-(2-(pent-4-en-1-yl)-1,3-dioxolan-2-yl)pentan-2-yl)oxy) diphenylsilane

There total 7 articles about (S)-tert-butyl((5-(2-(pent-4-en-1-yl)-1,3-dioxolan-2-yl)pentan-2-yl)oxy) diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1449688-78-1
(S)-10-((tert-butyldiphenylsilyl)oxy)undec-1-en-6-one

: 107-21-1
ethylene glycol

: 1449688-79-2
(S)-tert-butyl((5-(2-(pent-4-en-1-yl)-1,3-dioxolan-2-yl)pentan-2-yl)oxy) diphenylsilane

Guidance literature:: With toluene-4-sulfonic acid; In benzene; at 80 ℃;
DOI:10.1016/j.bmc.2013.06.024

Reference yield:

: 21889-88-3
hept-6-en-2-one

: 1449688-79-2
(S)-tert-butyl((5-(2-(pent-4-en-1-yl)-1,3-dioxolan-2-yl)pentan-2-yl)oxy) diphenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / ethanol / Reflux

2.1: n-butyllithium / tetrahydrofuran / 0 °C

2.2: 0 °C

3.1: toluene-4-sulfonic acid / benzene / 80 °C

With n-butyllithium; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; ethanol; benzene;
DOI:10.1016/j.bmc.2013.06.024

Reference yield:

: 143264-39-5
tert-butyl{[(1S)-1-methyl-2-propenyl]oxy}diphenylsilane

: 1449688-79-2
(S)-tert-butyl((5-(2-(pent-4-en-1-yl)-1,3-dioxolan-2-yl)pentan-2-yl)oxy) diphenylsilane

Guidance literature:: Multi-step reaction with 4 steps

1.1: 9-borabicyclo[3.3.1]nonane

2.1: 1H-imidazole; triphenylphosphine; iodine / 0 - 20 °C

3.1: n-butyllithium / tetrahydrofuran / 0 °C

3.2: 0 °C

4.1: toluene-4-sulfonic acid / benzene / 80 °C

With 1H-imidazole; n-butyllithium; iodine; toluene-4-sulfonic acid; 9-borabicyclo[3.3.1]nonane; triphenylphosphine; In tetrahydrofuran; benzene;
DOI:10.1016/j.bmc.2013.06.024