2-methoxy-4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

Base Information

Chemical Name:2-methoxy-4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate
CAS No.:304015-16-5
Molecular Formula:C₂₂H₃₀N₂O₆Si
Molecular Weight:446.575
Hs Code.:

Synonyms:2-methoxy-4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

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Chemical Property of 2-methoxy-4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

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Technology Process of 2-methoxy-4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

There total 2 articles about 2-methoxy-4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 131230-76-7
4-[(tert-butyldimethylsilyloxy)methyl]aniline

: 304015-15-4
2-methoxy-4-nitrobenzyl 4-nitrophenyl carbonate

: 304015-16-5
2-methoxy-4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

Guidance literature:: With 4 A molecular sieve; benzotriazol-1-ol; triethylamine; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1021/jm0205191

Reference yield:

: 136507-14-7
(2-methoxy-4-nitrophenyl)methanol

: 304015-16-5
2-methoxy-4-nitrobenzyl 4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ethyldiisopropylamine / tetrahydrofuran / 16 h / 20 °C

2: 77 percent / triethylamine; 1-hydroxybenzotriazole; molecular sieves 4 Angstroem / tetrahydrofuran / 16 h / 20 °C

With 4 A molecular sieve; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1016/j.bmc.2005.03.055