1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane

Base Information

Chemical Name:1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane
CAS No.:1566605-69-3
Molecular Formula:C₃₇H₅₃N₃O₁₀
Molecular Weight:699.842
Hs Code.:

Synonyms:1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane

Suppliers and Price of 1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane

There total 10 articles about 1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1566605-71-7
1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

: 146432-42-0
2-[bis(benzyloxycarbonylmethyl)amino]ethyl bromide

: 1566605-69-3
1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane

Guidance literature:: With potassium carbonate; In acetonitrile; at 60 ℃; for 72h;
DOI:10.1021/ol500022n

Reference yield:

: 146432-43-1
N-(2-bromoethyl)-N-[2-(1,1-dimethylethoxy)-2-oxoethyl]glycine 1,1-dimethylethyl ester

: 1566605-69-3
1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 16 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / isopropyl alcohol / 3 h / 20 °C

3: potassium carbonate / acetonitrile / 72 h / 60 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In isopropyl alcohol; acetonitrile;
DOI:10.1021/ol500022n

Reference yield:

: 1566605-91-1
1-methoxycarbonylmethyl-1-(4-nitrobenzenesulfonyl)-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

: 1566605-69-3
1,1-bis(benzyloxycarbonylmethyl)-4-methoxycarbonylmethyl-7,7-bis(tert-butoxycarbonylmethyl)-1,4,7-triazaheptane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; thiophenol / acetonitrile / 4 h / 20 °C

2: potassium carbonate / acetonitrile / 72 h / 60 °C

With potassium carbonate; thiophenol; In acetonitrile;
DOI:10.1021/ol500022n