meso-tri(4-methoxyphenyl)subporphyrin

Base Information

Chemical Name:meso-tri(4-methoxyphenyl)subporphyrin
CAS No.:945652-99-3
Molecular Formula:C₃₆H₂₈BN₃O₄
Molecular Weight:577.447
Hs Code.:

Synonyms:meso-tri(4-methoxyphenyl)subporphyrin

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Chemical Property of meso-tri(4-methoxyphenyl)subporphyrin

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Technology Process of meso-tri(4-methoxyphenyl)subporphyrin

There total 2 articles about meso-tri(4-methoxyphenyl)subporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 18899-90-6
tri(N-pyrrolyl)borane

: 123-11-5
4-methoxy-benzaldehyde

: 945652-99-3
meso-tri(4-methoxyphenyl)subporphyrin

Guidance literature:: In propionic acid; tripyrrolylborane was dispersed in propionic acid, the soln. was added slowly dropwise to a refluxing soln. of aldehyde in propionic acid over 45 min, heated under refluxed for a further 3-4 h; the solvent was removed, the residue was dissolved in CHCl3, passed through a short column of Celite, silica gel chromy. (CHCl3/CH3OH 30:1, 75:1v/v) and silica gel TLC (toluene/CH3OH 25:1 v/v, three times), HPLC (CH Cl3);
DOI:10.1021/ja0712120