10-(p-chlorophenyl)-4-hydrazinocyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine

Base Information

Chemical Name:10-(p-chlorophenyl)-4-hydrazinocyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine
CAS No.:345912-65-4
Molecular Formula:C₁₇H₁₃ClN₆S
Molecular Weight:368.849
Hs Code.:

Synonyms:10-(p-chlorophenyl)-4-hydrazinocyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine

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Chemical Property of 10-(p-chlorophenyl)-4-hydrazinocyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine

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Technology Process of 10-(p-chlorophenyl)-4-hydrazinocyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine

There total 5 articles about 10-(p-chlorophenyl)-4-hydrazinocyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 345912-64-3
4-chloro-10-(p-chlorophenyl)-cyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine

: 345912-65-4
10-(p-chlorophenyl)-4-hydrazinocyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine

Guidance literature:: With hydrazine hydrate; In ethanol; for 1h; Heating;
DOI:10.1080/10426500008076538

Reference yield:

: 134791-44-9
(E)-2-(4-chlorobenzylidene)cyclopentan-1-one

: 345912-65-4
10-(p-chlorophenyl)-4-hydrazinocyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / NaOMe / methanol / 48 h / 50 °C

2: 86 percent / AcONa*3H₂O / ethanol / 2 h / Heating

3: 90 percent / EtONa / ethanol / 0.08 h / Heating

4: 80 percent / NaNO₂; HCl; AcOH / H₂O / 2 h

5: 96 percent / NH₂NH₂*H₂O / ethanol / 1 h / Heating

With hydrogenchloride; sodium methylate; sodium ethanolate; sodium acetate; hydrazine hydrate; acetic acid; sodium nitrite; In methanol; ethanol; water; 3: Thorpe-Ziegler cyclization;
DOI:10.1080/10426500008076538

Reference yield:

: 83236-50-4
4-<4-chlorophenyl>-3-cyano-5,6-trimethylenepyridine-2<1H>-thione

: 345912-65-4
10-(p-chlorophenyl)-4-hydrazinocyclopenta[5',6']pyrido[3',2':4,5]thieno-[3,2-d]-[1,2,3]triazine

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / AcONa*3H₂O / ethanol / 2 h / Heating

2: 90 percent / EtONa / ethanol / 0.08 h / Heating

3: 80 percent / NaNO₂; HCl; AcOH / H₂O / 2 h

4: 96 percent / NH₂NH₂*H₂O / ethanol / 1 h / Heating

With hydrogenchloride; sodium ethanolate; sodium acetate; hydrazine hydrate; acetic acid; sodium nitrite; In ethanol; water; 2: Thorpe-Ziegler cyclization;
DOI:10.1080/10426500008076538