({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester

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Chemical Name:({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester
CAS No.:185670-58-0
Molecular Formula:C₄₁H₄₃N₄O₁₀P
Molecular Weight:782.787
Hs Code.:

({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester

Synonyms:({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester

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Chemical Property of ({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester

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Technology Process of ({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester

There total 6 articles about ({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107-18-6
allyl alcohol

: 183057-87-6
({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid mono-[2-(4-nitro-phenyl)-ethyl] ester

: 185670-58-0
({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester

Guidance literature:: With 1-(toluene-p-sulphonyl)-3-nitro-1,2,4-triazole; In pyridine;

Reference yield:

: 20924-05-4
thymidyl acetic acid

: 185670-58-0
({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / HOBT, N-ethylmorpholine, diisopropylcarbodiimide / dimethylformamide / 16 h / Ambient temperature

2: 90 percent / 0.1 M DBU / pyridine / 4 h

3: 95 percent / 3-nitro-1-(p-toluenesulfonyl)-1H-1,2,4-triazole / pyridine

With N-ethylmorpholine;; benzotriazol-1-ol; 1-(toluene-p-sulphonyl)-3-nitro-1,2,4-triazole; 1,8-diazabicyclo[5.4.0]undec-7-ene; diisopropyl-carbodiimide; In pyridine; N,N-dimethyl-formamide;

Reference yield:

: 183057-37-6
2-Amino-1-(4-methoxytriphenylmethoxy)ethane

: 185670-58-0
({{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-methyl)-phosphonic acid allyl ester 2-(4-nitro-phenyl)-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 55 percent / methanol / 4 h / Ambient temperature

2: 60 percent / 0.5 h / 100 °C

3: 90 percent / HOBT, N-ethylmorpholine, diisopropylcarbodiimide / dimethylformamide / 16 h / Ambient temperature

4: 90 percent / 0.1 M DBU / pyridine / 4 h

5: 95 percent / 3-nitro-1-(p-toluenesulfonyl)-1H-1,2,4-triazole / pyridine

With N-ethylmorpholine;; benzotriazol-1-ol; 1-(toluene-p-sulphonyl)-3-nitro-1,2,4-triazole; 1,8-diazabicyclo[5.4.0]undec-7-ene; diisopropyl-carbodiimide; In pyridine; methanol; N,N-dimethyl-formamide;