3-(4-fluorophenyl)-4-(4-methoxyphenyl)-1-phenyl-4H,6H-thiazolo[3,4-a]pyrazoloimidazole

Base Information

Chemical Name:3-(4-fluorophenyl)-4-(4-methoxyphenyl)-1-phenyl-4H,6H-thiazolo[3,4-a]pyrazoloimidazole
CAS No.:1338328-71-4
Molecular Formula:C₂₅H₁₉FN₄OS
Molecular Weight:442.516
Hs Code.:

Synonyms:3-(4-fluorophenyl)-4-(4-methoxyphenyl)-1-phenyl-4H,6H-thiazolo[3,4-a]pyrazoloimidazole

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Chemical Property of 3-(4-fluorophenyl)-4-(4-methoxyphenyl)-1-phenyl-4H,6H-thiazolo[3,4-a]pyrazoloimidazole

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Technology Process of 3-(4-fluorophenyl)-4-(4-methoxyphenyl)-1-phenyl-4H,6H-thiazolo[3,4-a]pyrazoloimidazole

There total 4 articles about 3-(4-fluorophenyl)-4-(4-methoxyphenyl)-1-phenyl-4H,6H-thiazolo[3,4-a]pyrazoloimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1338328-65-6
3-(4-fluorophenyl)-1-phenyl-1H-pyrazole-4,5-diamine

: 123-11-5
4-methoxy-benzaldehyde

: 68-11-1
mercaptoacetic acid

: 1338328-71-4
3-(4-fluorophenyl)-4-(4-methoxyphenyl)-1-phenyl-4H,6H-thiazolo[3,4-a]pyrazoloimidazole

Guidance literature:: In benzene; at 160 ℃; for 0.333333h; Microwave irradiation;
DOI:10.1002/cjoc.201180265

Reference yield:

: 72411-53-1
3-(4-fluorophenyl)-1-phenyl-1H-pyrazol-5-amine

: 1338328-71-4
3-(4-fluorophenyl)-4-(4-methoxyphenyl)-1-phenyl-4H,6H-thiazolo[3,4-a]pyrazoloimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; sodium nitrite / water / 0 - 20 °C

2: hydrogenchloride; tin(ll) chloride / water / 0.25 h / 0 - 20 °C

3: benzene / 0.33 h / 160 °C / Microwave irradiation

With hydrogenchloride; tin(ll) chloride; sodium nitrite; In water; benzene;
DOI:10.1002/cjoc.201180265

Reference yield:

: 1338328-62-3
3-(4-fluorophenyl)-1-phenyl-4-(phenyldiazenyl)-1H-pyrazol-5-amine

: 1338328-71-4
3-(4-fluorophenyl)-4-(4-methoxyphenyl)-1-phenyl-4H,6H-thiazolo[3,4-a]pyrazoloimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium dithionite / ethanol; water / Heating

2: benzene / 0.33 h / 160 °C / Microwave irradiation

With sodium dithionite; In ethanol; water; benzene;
DOI:10.1002/cjoc.201180265