N-(3-Chloro-phenyl)-N'-[1-(4-methoxy-phenyl)-eth-(E)-ylidene]-hydrazine

Base Information

Chemical Name:N-(3-Chloro-phenyl)-N'-[1-(4-methoxy-phenyl)-eth-(E)-ylidene]-hydrazine
CAS No.:109793-40-0
Molecular Formula:C₁₅H₁₅ClN₂O
Molecular Weight:274.75
Hs Code.:

Synonyms:N-(3-Chloro-phenyl)-N'-[1-(4-methoxy-phenyl)-eth-(E)-ylidene]-hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-Chloro-phenyl)-N'-[1-(4-methoxy-phenyl)-eth-(E)-ylidene]-hydrazine

Chemical Property:

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Technology Process of N-(3-Chloro-phenyl)-N'-[1-(4-methoxy-phenyl)-eth-(E)-ylidene]-hydrazine

There total 2 articles about N-(3-Chloro-phenyl)-N'-[1-(4-methoxy-phenyl)-eth-(E)-ylidene]-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 14763-20-3
3-chlorophenyl hydrazine

: 109793-40-0
N-(3-Chloro-phenyl)-N'-[1-(4-methoxy-phenyl)-eth-(E)-ylidene]-hydrazine

Guidance literature:: acetic acid; In ethanol; Heating;
DOI:10.1016/0223-5234(87)90010-9

Reference yield:

: 2312-23-4
m-chlorophenylhydrazine hydrochloride

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 109793-40-0
N-(3-Chloro-phenyl)-N'-[1-(4-methoxy-phenyl)-eth-(E)-ylidene]-hydrazine

Guidance literature:: With sodium acetate; In ethanol; for 6h; Reflux;

Reference yield:

: 109793-40-0
N-(3-Chloro-phenyl)-N'-[1-(4-methoxy-phenyl)-eth-(E)-ylidene]-hydrazine

: 1422538-47-3
3-[1-(3-chlorophenyl)-3-(4-methoxyphenyl)-1H-pyrazol-4-yl]-4,5-dihydro-5-oxo-1H-pyrazol-4-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 0.5 h / 0 °C

1.2: 15 h / 0 °C

2.1: acetic acid / ethanol / Reflux

With acetic acid; trichlorophosphate; In ethanol; 1.1: Vilsmeier-Haack reaction;