N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine

Base Information

Chemical Name:N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine
CAS No.:1041862-64-9
Molecular Formula:C₅₅H₇₄Br₂N₄O₅
Molecular Weight:1031.02
Hs Code.:

Synonyms:N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine

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Chemical Property of N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine

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Technology Process of N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine

There total 1 articles about N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 473269-70-4
5-tert-butyl-2-methoxybenzene-1,3-diamine

: 132268-08-7
1,3-dibromo-5-(tert-butyl)-2-methoxybenzene

: 854669-22-0
N,N'-bis(3-bromo-5-tert-butyl-2-methoxyphenyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

: 1041862-64-9
N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine

Guidance literature:: With palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In toluene; at 80 ℃; for 17h; Inert atmosphere;
DOI:10.1039/b801127c

Reference yield: 92.0%

: 1041862-64-9
N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine

: 100-39-0
benzyl bromide

: 1048983-41-0
C₈₃H₉₈Br₂N₄O₅

Guidance literature:: N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200800502

Reference yield: 87.0%

: 1041862-64-9
N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine

: 74-88-4
methyl iodide

: 1041862-63-8
N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxy-N''-methylanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-N,N'-dimethyl-1,3-phenylenediamine

Guidance literature:: N,N'-bis[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tert-butyl-2-methoxyphenyl]-5-tert-butyl-2-methoxy-1,3-phenylenediamine; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.166667h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; Inert atmosphere;
DOI:10.1039/b801127c