Phenylbiphenyl-2,2'-ylenebismuth diacetate

Base Information

• Chemical Name: Phenylbiphenyl-2,2'-ylenebismuth diacetate
• CAS No.: 325723-04-4
• Molecular Formula: C₂₂H₁₉BiO₄
• Molecular Weight: 556.371
• Mol file: 325723-04-4.mol

Synonyms:Phenylbiphenyl-2,2'-ylenebismuth diacetate

Chemical Property of Phenylbiphenyl-2,2'-ylenebismuth diacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phenylbiphenyl-2,2'-ylenebismuth diacetate

There total 1 articles about Phenylbiphenyl-2,2'-ylenebismuth diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic acid (64-19-7,77671-22-8) + phenylbiphenyl-2,2'-ylenebismuthane (41137-17-1) → Phenylbiphenyl-2,2'-ylenebismuth diacetate (325723-04-4)

Guidance literature:

With peracetic acid; In tetrahydrofuran; dichloromethane; 0 °C, 0.5 h;

DOI:10.1246/cl.2007.718

Reference yield: 96.0%

piperidine (110-89-4) + Phenylbiphenyl-2,2'-ylenebismuth diacetate (325723-04-4) → N-phenyl piperidine (4096-20-2)

Guidance literature:

With copper diacetate; In tetrahydrofuran; at 50 ℃; for 3h;

DOI:10.1039/b006307j

Reference yield: 95.0%

ethyl 2-oxocyclohexane carboxylate (1655-07-8) + Phenylbiphenyl-2,2'-ylenebismuth diacetate (325723-04-4) → ethyl 2-oxo-1-phenylcyclohexane-1-carboxylate (38691-00-8,38691-01-9,55285-81-9)

Guidance literature:

With N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; at 20 ℃; for 17h;

DOI:10.1039/b006307j

upstream raw materials:

acetic acid

phenylbiphenyl-2,2'-ylenebismuthane

Downstream raw materials:

N-phenyl piperidine

2-phenyl-1,2,3,4-tetrahydroisoquinoline

N-(3,4-Dimethylphenyl)-N-phenylamine

N-tert-butylaniline

Refernces