phenylbiphenyl-2,2'-ylenebismuthane

Base Information

Chemical Name:phenylbiphenyl-2,2'-ylenebismuthane
CAS No.:41137-17-1
Molecular Formula:C₁₈H₁₃Bi
Molecular Weight:438.282
Hs Code.:

Synonyms:phenylbiphenyl-2,2'-ylenebismuthane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylbiphenyl-2,2'-ylenebismuthane

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Technology Process of phenylbiphenyl-2,2'-ylenebismuthane

There total 5 articles about phenylbiphenyl-2,2'-ylenebismuthane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 13029-09-9
2,2'-dibromobiphenyl

: 603-33-8
triphenylbismuthane

: 41137-17-1
phenylbiphenyl-2,2'-ylenebismuthane

Guidance literature:: 2,2'-dibromobiphenyl; With n-butyllithium; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

triphenylbismuthane; With bismuth(III) chloride; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; Inert atmosphere;

Reference yield: 72.0%

: 39110-03-7
diiodo(phenyl)bismuth(III)

: 16291-32-0
biphenyl-2,2'-diyl-bis-lithium

: 41137-17-1
phenylbiphenyl-2,2'-ylenebismuthane

Guidance literature:: In tetrahydrofuran; diethyl ether; 90 min reacn. with freshy prepared 2,2'-dilithium bihhenyl; treatment with H2O, evapn. of ether phase;