{6-[2-(3,5-dichloropyridin-4-yl)acetyl]-2,3-dimethoxyphenoxy}aceticacid

Base Information

Chemical Name:{6-[2-(3,5-dichloropyridin-4-yl)acetyl]-2,3-dimethoxyphenoxy}aceticacid
CAS No.:1035572-31-6
Molecular Formula:C₁₇H₁₅Cl₂NO₆
Molecular Weight:400.215
Hs Code.:

Synonyms:{6-[2-(3,5-dichloropyridin-4-yl)acetyl]-2,3-dimethoxyphenoxy}aceticacid

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Chemical Property of {6-[2-(3,5-dichloropyridin-4-yl)acetyl]-2,3-dimethoxyphenoxy}aceticacid

Chemical Property:

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Technology Process of {6-[2-(3,5-dichloropyridin-4-yl)acetyl]-2,3-dimethoxyphenoxy}aceticacid

There total 4 articles about {6-[2-(3,5-dichloropyridin-4-yl)acetyl]-2,3-dimethoxyphenoxy}aceticacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100868-46-0
3,5-dichloro-4-picoline

: 1035572-31-6
{6-[2-(3,5-dichloropyridin-4-yl)acetyl]-2,3-dimethoxyphenoxy}aceticacid

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.5 h / 0 °C

2.1: boron trichloride / dichloromethane / 2 h / 20 °C

3.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 20 °C

4.1: lithium hydroxide / methanol; water / 1 h / 20 °C

4.2: pH 1

With boron trichloride; potassium carbonate; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; water;
DOI:10.1021/jm500378a

Reference yield:

: 1035571-27-7
2-(3,5-dichloro-4-pyridinyl)-1-(2-hydroxy-3,4-dimethoxyphenyl)ethanone

: 1035572-31-6
{6-[2-(3,5-dichloropyridin-4-yl)acetyl]-2,3-dimethoxyphenoxy}aceticacid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 20 °C

2.1: lithium hydroxide / methanol; water / 1 h / 20 °C

2.2: pH 1

With potassium carbonate; lithium hydroxide; In 1-methyl-pyrrolidin-2-one; methanol; water;
DOI:10.1021/jm500378a

Reference yield:

: 208043-54-3
[2-(3,5-Dichloro-pyridin-4-yl)-1-oxoethyl]-2,3,4-trimethoxybenzene

: 1035572-31-6
{6-[2-(3,5-dichloropyridin-4-yl)acetyl]-2,3-dimethoxyphenoxy}aceticacid

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trichloride / dichloromethane / 2 h / 20 °C

2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 20 °C

3.1: lithium hydroxide / methanol; water / 1 h / 20 °C

3.2: pH 1

With boron trichloride; potassium carbonate; lithium hydroxide; In 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; water;
DOI:10.1021/jm500378a