triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate

Base Information

• Chemical Name: triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate
• CAS No.: 1083039-03-5
• Molecular Formula: C₂₃H₂₈I₄O₄Si
• Molecular Weight: 904.176

Synonyms:triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate

Chemical Property of triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate

Chemical Property:

Purity/Quality:

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Technology Process of triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate

There total 2 articles about triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

triisopropylsilyl chloride (13154-24-0) + tetrac (67-30-1) → triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate (1083039-03-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.bmcl.2009.04.094

Reference yield:

triisopropylsilyl chloride (13154-24-0) → triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate (1083039-03-5)

Guidance literature:

With triethanolamine; In tetrahydrofuran;

Reference yield: 47.0%

triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate (1083039-03-5) + 1,2-Epoxy-3-bromopropane (3132-64-7,82584-73-4) → oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate (1174546-80-5) + triisopropylsilyl 2-(4-(3,5-diiodo-4-(oxiran-2-ylmethoxy)phenoxy)-3,5-diiodophenyl)acetate (1174546-78-1)

Guidance literature:

With triethylamine; at 55 ℃; for 0.5h; Time; Kinetics; Inert atmosphere;

upstream raw materials:

triisopropylsilyl chloride

tetrac

Downstream raw materials:

oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate

N-cyclohexyl-2-(4-(3,5-diiodo-4-(oxiran-2-ylmethoxy)phenoxy)-3,5-diiodophenyl)acetamide

{4-[3,5-diiodo-4-(oxiran-2-ylmethoxy)phenoxy]-3,5-diiodophenyl}acetic acidn

N-cyclohexyl-2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetamide

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