oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate

Base Information

Chemical Name:oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate
CAS No.:1174546-80-5
Molecular Formula:C₂₀H₁₆I₄O₆
Molecular Weight:859.961
Hs Code.:

Synonyms:oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate

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Chemical Property of oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate

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Technology Process of oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate

There total 3 articles about oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1083039-03-5
triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate

: 3132-64-7,82584-73-4
1,2-Epoxy-3-bromopropane

: 1174546-80-5
oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate

: 1174546-78-1
triisopropylsilyl 2-(4-(3,5-diiodo-4-(oxiran-2-ylmethoxy)phenoxy)-3,5-diiodophenyl)acetate

Guidance literature:: With triethylamine; at 55 ℃; for 0.5h; Time; Kinetics; Inert atmosphere;

Reference yield: 25.5%

: 1083039-03-5
triisopropylsilyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate

: 3132-64-7,82584-73-4
1,2-Epoxy-3-bromopropane

: 1174546-80-5
oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 55 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmcl.2009.04.094

Reference yield:

: 67-30-1
tetrac

: 1174546-80-5
oxiran-2-ylmethyl 2-(4-(3,5-diiodo-4-(oxiran-2-yl)methoxyphenoxy)-3,5-diiodophenyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 0.08 h / 20 °C

1.2: 0.33 h

2.1: triethylamine / tetrahydrofuran / 0.08 h / 20 °C

2.2: 12 h / Reflux

With triethylamine; In tetrahydrofuran;