2-methoxycyclohexanone oxime

Base Information

• Chemical Name: 2-methoxycyclohexanone oxime
• CAS No.: 3307-32-2
• Molecular Formula: C₇H₁₃NO₂
• Molecular Weight: 143.186

Synonyms:2-methoxycyclohexanone oxime

Chemical Property of 2-methoxycyclohexanone oxime

Chemical Property:

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Technology Process of 2-methoxycyclohexanone oxime

There total 2 articles about 2-methoxycyclohexanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-methoxycyclohexanone (7429-44-9) → 2-methoxycyclohexanone oxime (3307-32-2)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In methanol; water; at 70 ℃; for 16h; Sealed tube;

Reference yield:

sodium methylate (124-41-4) + cyclohexene (110-83-8) → 2-methoxycyclohexanone oxime (3307-32-2)

Guidance literature:

Multistep reaction; (i) NOCl, HCl, (ii) /BRN= 3592982/, MeOH;

DOI:10.1246/bcsj.39.1119

Reference yield: 100.0%

2-methoxycyclohexanone oxime (3307-32-2) + acetic anhydride (108-24-7) → C9H15NO3 (137936-34-6)

Guidance literature:

With pyridine;

DOI:10.1039/c39910000533

upstream raw materials:

2-methoxycyclohexanone

sodium methylate

cyclohexene

Downstream raw materials:

6-Methoxy-8-oxo-8-phenyl-octanenitrile

C₉H₁₅NO₃

2-methoxy-phenylamine

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