2-ethenyl-6-p-nitrophenoxymethyloxymethylpyridine

Base Information

• Chemical Name: 2-ethenyl-6-p-nitrophenoxymethyloxymethylpyridine
• CAS No.: 112936-15-9
• Molecular Formula: C₁₆H₁₄N₂O₅
• Molecular Weight: 314.298
• Mol file: 112936-15-9.mol

Synonyms:2-ethenyl-6-p-nitrophenoxymethyloxymethylpyridine

Chemical Property of 2-ethenyl-6-p-nitrophenoxymethyloxymethylpyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-ethenyl-6-p-nitrophenoxymethyloxymethylpyridine

There total 6 articles about 2-ethenyl-6-p-nitrophenoxymethyloxymethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methanoyl-6-methoxycarbonylmethoxymethylpyridine (114832-60-9) → 2-ethenyl-6-p-nitrophenoxymethyloxymethylpyridine (112936-15-9)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran

2: LiOH / H₂O; methanol

3: dicyclohexylcarbodiimide / CH₂Cl₂

With lithium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1039/c39880000156

Reference yield:

2-hydroxymethyl-6-methoxycarbonylmethoxymethylpyridine (114832-59-6) → 2-ethenyl-6-p-nitrophenoxymethyloxymethylpyridine (112936-15-9)

Guidance literature:

Multi-step reaction with 4 steps

1: MnO₂ / CH₂Cl₂

2: tetrahydrofuran

3: LiOH / H₂O; methanol

4: dicyclohexylcarbodiimide / CH₂Cl₂

With manganese(IV) oxide; lithium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1039/c39880000156

Reference yield:

2.6-bis(hydroxymethyl)pyridine (1195-59-1) → 2-ethenyl-6-p-nitrophenoxymethyloxymethylpyridine (112936-15-9)

Guidance literature:

Multi-step reaction with 5 steps

1: NaH / tetrahydrofuran

2: MnO₂ / CH₂Cl₂

3: tetrahydrofuran

4: LiOH / H₂O; methanol

5: dicyclohexylcarbodiimide / CH₂Cl₂

With manganese(IV) oxide; lithium hydroxide; sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1039/c39880000156

upstream raw materials:

4-nitro-phenol

2-ethenyl-6-methoxycarbonylmethyloxymethylpyridine

(6-Vinyl-pyridin-2-ylmethoxy)-acetic acid

2.6-bis(hydroxymethyl)pyridine

Downstream raw materials:

<4-(1,4,7,10-tetra-azacyclotridecan-12-ylmethyl)benzylcarbamoylmethoxymethyl>pyridine

2-ethenyl-6-<4-hydroxy-3-(1,4,7,10-tetra-azacyclotridecan-11-yl-benzyl)carbamoylmethoxymethyl>pyridine

2-ethenyl-6-<4-(1,4,8,11-tetra-azacyclotetradecan-6-ylmethyl)benzylcarbamoylmethoxymethyl>pyridine

2-ethenyl-6-<4-hydroxy-3-(1,4,8,11-tetra-azacyclotetradecan-5-yl)benzylcarbamoylmethoxymethyl>pyridine