(3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

Base Information

Chemical Name:(3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide
CAS No.:868127-82-6
Molecular Formula:C₂₈H₄₀O₅Si
Molecular Weight:484.708
Hs Code.:

Synonyms:(3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

Suppliers and Price of (3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

Chemical Property:

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Technology Process of (3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

There total 2 articles about (3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₄₂O₅Si

: 868127-82-6
(3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/np050089s

Reference yield:

: C₂₈H₄₂O₅Si

: 868127-82-6
(3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

: 868127-81-5
(3R)-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 16h; Title compound not separated from byproducts.;
DOI:10.1021/np050089s

Reference yield: 81.0%

: 868127-82-6
(3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 868127-84-8
(2S,3R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-3-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

Guidance literature:: (3R)-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -70 ℃;

3-methoxy-4-(phenylmethoxy)benzaldehyde; In tetrahydrofuran; toluene; at -70 ℃; for 1h; Further stages.;
DOI:10.1021/np050089s