Technology Process of C35H40O8S
There total 6 articles about C35H40O8S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene / 46 h / 70 °C / Inert atmosphere
2: 5%-palladium/activated carbon; hydrogen / n-heptane; ethyl acetate / 0.33 h / Inert atmosphere
3: potassium carbonate / 15 h / -78 °C
With
5%-palladium/activated carbon; hydrogen; potassium carbonate;
In
n-heptane; ethyl acetate; toluene;
DOI:10.1016/j.tetlet.2014.02.069
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 1.5 h / Reflux; Inert atmosphere
2: toluene / 46 h / 70 °C / Inert atmosphere
3: 5%-palladium/activated carbon; hydrogen / n-heptane; ethyl acetate / 0.33 h / Inert atmosphere
4: potassium carbonate / 15 h / -78 °C
With
5%-palladium/activated carbon; 2-chloro-1-methyl-pyridinium iodide; hydrogen; potassium carbonate; triethylamine;
In
n-heptane; dichloromethane; ethyl acetate; toluene;
DOI:10.1016/j.tetlet.2014.02.069