methyl 5-hydroxy-2-mesityl-5-methyl-3-oxo-7-(4-(trifluoromethyl) phenylthio)heptanoate

Base Information

Chemical Name:methyl 5-hydroxy-2-mesityl-5-methyl-3-oxo-7-(4-(trifluoromethyl) phenylthio)heptanoate
CAS No.:1612831-55-6
Molecular Formula:C₂₅H₂₉F₃O₄S
Molecular Weight:482.564
Hs Code.:

Synonyms:methyl 5-hydroxy-2-mesityl-5-methyl-3-oxo-7-(4-(trifluoromethyl) phenylthio)heptanoate

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Chemical Property of methyl 5-hydroxy-2-mesityl-5-methyl-3-oxo-7-(4-(trifluoromethyl) phenylthio)heptanoate

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Technology Process of methyl 5-hydroxy-2-mesityl-5-methyl-3-oxo-7-(4-(trifluoromethyl) phenylthio)heptanoate

There total 3 articles about methyl 5-hydroxy-2-mesityl-5-methyl-3-oxo-7-(4-(trifluoromethyl) phenylthio)heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1044064-34-7
4-(4-(trifluoromethyl)phenylthio)butan-2-one

: 1612831-46-5
methyl 2-mesityl-3-oxobutanoate

: 1612831-55-6
methyl 5-hydroxy-2-mesityl-5-methyl-3-oxo-7-(4-(trifluoromethyl) phenylthio)heptanoate

Guidance literature:: methyl 2-mesityl-3-oxobutanoate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

With n-butyllithium; In tetrahydrofuran; at -40 ℃; for 0.5h;

4-(4-(trifluoromethyl)phenylthio)butan-2-one; In tetrahydrofuran; at -40 ℃; for 0.5h;

Reference yield:

: 825-83-2
4-trifluoromethylbenzenethiol

: 1612831-55-6
methyl 5-hydroxy-2-mesityl-5-methyl-3-oxo-7-(4-(trifluoromethyl) phenylthio)heptanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 16 h / 10 - 30 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

2.2: 0.5 h / -40 °C

2.3: 0.5 h / -40 °C

With sodium hydride; potassium carbonate; In tetrahydrofuran; acetonitrile;

Reference yield:

: 41841-19-4
methyl 2-mesitylacetate

: 1612831-55-6
methyl 5-hydroxy-2-mesityl-5-methyl-3-oxo-7-(4-(trifluoromethyl) phenylthio)heptanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 7 h / -78 - 30 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

2.2: 0.5 h / -40 °C

2.3: 0.5 h / -40 °C

With sodium hydride; lithium diisopropyl amide; In tetrahydrofuran;