Technology Process of 1-ethenyl-1-methoxycyclohexane
There total 3 articles about 1-ethenyl-1-methoxycyclohexane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1-vinylcyclohexanol;
With
sodium hydride;
In
tetrahydrofuran;
for 2h;
Heating;
dimethyl sulfate;
In
tetrahydrofuran;
Heating;
DOI:10.1007/s00706-004-0163-0
- Guidance literature:
-
1-vinylcyclohexanol;
With
sodium hydride;
In
tetrahydrofuran;
at 0 ℃;
for 0.5h;
methyl iodide;
In
tetrahydrofuran;
at 20 - 40 ℃;
for 22h;
methyl iodide;
With
sodium hydride;
In
tetrahydrofuran;
at 0 - 40 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 66 percent / tetrahydrofuran; diethyl ether / -5 - 20 °C
2.1: NaH / tetrahydrofuran / 2 h / Heating
2.2: 81 percent / tetrahydrofuran / Heating
With
sodium hydride;
In
tetrahydrofuran; diethyl ether;
DOI:10.1007/s00706-004-0163-0
