hydrogen (3R)-1-methyl 3-[(tert-butyldimethylsilyl)-oxy]pentanedioate cyclohexylamine salt

Base Information

Chemical Name:hydrogen (3R)-1-methyl 3-[(tert-butyldimethylsilyl)-oxy]pentanedioate cyclohexylamine salt
CAS No.:1350364-00-9
Molecular Formula:C₆H₁₃N*C₁₂H₂₄O₅Si
Molecular Weight:375.581
Hs Code.:

Synonyms:hydrogen (3R)-1-methyl 3-[(tert-butyldimethylsilyl)-oxy]pentanedioate cyclohexylamine salt

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hydrogen (3R)-1-methyl 3-[(tert-butyldimethylsilyl)-oxy]pentanedioate cyclohexylamine salt

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of hydrogen (3R)-1-methyl 3-[(tert-butyldimethylsilyl)-oxy]pentanedioate cyclohexylamine salt

There total 1 articles about hydrogen (3R)-1-methyl 3-[(tert-butyldimethylsilyl)-oxy]pentanedioate cyclohexylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 109744-49-2
Hydrogen (3R)-1-methyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate

: 1350364-00-9
hydrogen (3R)-1-methyl 3-[(tert-butyldimethylsilyl)-oxy]pentanedioate cyclohexylamine salt

Guidance literature:: In hexane; for 3.33333h;

Reference yield:

: 1350364-00-9
hydrogen (3R)-1-methyl 3-[(tert-butyldimethylsilyl)-oxy]pentanedioate cyclohexylamine salt

: 109744-49-2
Hydrogen (3R)-1-methyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate

Guidance literature:: With hydrogenchloride; In dichloromethane; water; at 15 - 20 ℃;

Reference yield:

: 1350364-00-9
hydrogen (3R)-1-methyl 3-[(tert-butyldimethylsilyl)-oxy]pentanedioate cyclohexylamine salt

: 147118-35-2
methyl (3R)-3-(tert-butyldimethylsilyloxy)-5-oxo-6-triphenylphosphoranylidenehexanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / dichloromethane; water / 15 - 20 °C

2.1: triethylamine / hexane / 3 h / -40 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / 0 °C

3.2: 3 h / -78 °C

With hydrogenchloride; n-butyllithium; triethylamine; In tetrahydrofuran; hexane; dichloromethane; water;