Technology Process of tetradec-2-enedioic acid 14-benzyl ester
There total 6 articles about tetradec-2-enedioic acid 14-benzyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 8.50 g / KHCO3 / dimethylformamide / 24 h / 20 °C
2.1: 3.15 g / pyridinium chlorochromate / CH2Cl2 / 1.5 h / 20 °C
3.1: NaH / tetrahydrofuran / 0 °C
3.2: 9.80 g / tetrahydrofuran / 24 h
4.1: 3.95 g / p-toluenesulfonic acid / toluene
With
sodium hydride; potassium hydrogencarbonate; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja035558w
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 3.15 g / pyridinium chlorochromate / CH2Cl2 / 1.5 h / 20 °C
2.1: NaH / tetrahydrofuran / 0 °C
2.2: 9.80 g / tetrahydrofuran / 24 h
3.1: 3.95 g / p-toluenesulfonic acid / toluene
With
sodium hydride; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja035558w
