tetradec-2-enedioic acid 14-benzyl ester

Base Information

Chemical Name:tetradec-2-enedioic acid 14-benzyl ester
CAS No.:341925-16-4
Molecular Formula:C₂₁H₃₀O₄
Molecular Weight:346.467
Hs Code.:

Synonyms:tetradec-2-enedioic acid 14-benzyl ester

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Chemical Property of tetradec-2-enedioic acid 14-benzyl ester

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Technology Process of tetradec-2-enedioic acid 14-benzyl ester

There total 6 articles about tetradec-2-enedioic acid 14-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 341925-15-3
tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester

: 341925-16-4
tetradec-2-enedioic acid 14-benzyl ester

Guidance literature:: With toluene-4-sulfonic acid; In toluene;
DOI:10.1021/ja035558w

Reference yield:

: 505-95-3
12-hydroxydodecanoic acid

: 341925-16-4
tetradec-2-enedioic acid 14-benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 8.50 g / KHCO₃ / dimethylformamide / 24 h / 20 °C

2.1: 3.15 g / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / 20 °C

3.1: NaH / tetrahydrofuran / 0 °C

3.2: 9.80 g / tetrahydrofuran / 24 h

4.1: 3.95 g / p-toluenesulfonic acid / toluene

With sodium hydride; potassium hydrogencarbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja035558w

Reference yield:

: 99837-97-5
benzyl 12-hydroxydodecanoate

: 341925-16-4
tetradec-2-enedioic acid 14-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3.15 g / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / 20 °C

2.1: NaH / tetrahydrofuran / 0 °C

2.2: 9.80 g / tetrahydrofuran / 24 h

3.1: 3.95 g / p-toluenesulfonic acid / toluene

With sodium hydride; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja035558w