tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester

Base Information

Chemical Name:tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester
CAS No.:341925-15-3
Molecular Formula:C₂₅H₃₈O₄
Molecular Weight:402.574
Hs Code.:

Synonyms:tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester

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Chemical Property of tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester

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Technology Process of tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester

There total 5 articles about tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62327-21-3
tert-butyl dimethylphosphonoacetate

: 341925-14-2
12-oxo-dodecanoic acid benzyl ester

: 341925-15-3
tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester

Guidance literature:: tert-butyl dimethylphosphonoacetate; With sodium hydride; In tetrahydrofuran; at 0 ℃;

12-oxo-dodecanoic acid benzyl ester; In tetrahydrofuran; for 24h;
DOI:10.1021/ja035558w

Reference yield:

: 505-95-3
12-hydroxydodecanoic acid

: 341925-15-3
tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 8.50 g / KHCO₃ / dimethylformamide / 24 h / 20 °C

2.1: 3.15 g / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / 20 °C

3.1: NaH / tetrahydrofuran / 0 °C

3.2: 9.80 g / tetrahydrofuran / 24 h

With sodium hydride; potassium hydrogencarbonate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja035558w

Reference yield:

: 99837-97-5
benzyl 12-hydroxydodecanoate

: 341925-15-3
tetradec-2-enedioic acid 14-benzyl ester 1-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3.15 g / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / 20 °C

2.1: NaH / tetrahydrofuran / 0 °C

2.2: 9.80 g / tetrahydrofuran / 24 h

With sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja035558w