2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde ethylene acetal

Base Information

Chemical Name:2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde ethylene acetal
CAS No.:1374113-84-4
Molecular Formula:C₂₅H₁₅F₁₂O₂P
Molecular Weight:606.347
Hs Code.:

Synonyms:2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde ethylene acetal

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Chemical Property of 2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde ethylene acetal

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Technology Process of 2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde ethylene acetal

There total 1 articles about 2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 34824-58-3
2-(2-bromophenyl)-1,3-dioxolan

: 142421-57-6
bis(3,5-di(trifluoromethyl)phenyl)chlorophosphine

: 1374113-84-4
2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde ethylene acetal

Guidance literature:: 2-(2-bromophenyl)-1,3-dioxolan; With tert.-butyl lithium; In diethyl ether; at -78 ℃; for 1h;

bis(3,5-di(trifluoromethyl)phenyl)chlorophosphine; In diethyl ether; at -78 - 20 ℃;
DOI:10.1021/jo300548z

Reference yield: 82.0%

: 1374113-84-4
2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde ethylene acetal

: 67-64-1
acetone

: 1374113-87-7
2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde

Guidance literature:: With water; toluene-4-sulfonic acid; Reflux;
DOI:10.1021/jo300548z

Reference yield:

: 1374113-84-4
2-(di-3,5-bistrifluoromethylphenylphosphino)benzaldehyde ethylene acetal

: 1374113-90-2
(2S,5S)-1-[2-(di-3,5-bistrifluoromethyphenylphosphino)benzylideneamino]-2,5-diphenylpyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: water; toluene-4-sulfonic acid / Reflux

2: toluene / 3 h / 20 °C

With water; toluene-4-sulfonic acid; In toluene;
DOI:10.1021/jo300548z