Technology Process of C17H10BrN3O
There total 5 articles about C17H10BrN3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; oxygen; copper diacetate;
In
dimethyl sulfoxide;
at 40 - 50 ℃;
for 96h;
DOI:10.1021/jm301268u
- Guidance literature:
-
Multi-step reaction with 5 steps
1: n-butyllithium; Trimethyl borate / tetrahydrofuran / -75.1 - 20 °C / Inert atmosphere
2: potassium carbonate; palladium diacetate; triphenylphosphine / water; 1,2-dimethoxyethane / 5.67 h / Reflux
3: hydrogenchloride / water / 3 h / Reflux
4: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 20 °C
5: copper diacetate; pyridine; oxygen / dimethyl sulfoxide / 96 h / 40 - 50 °C
With
pyridine; hydrogenchloride; N-Bromosuccinimide; n-butyllithium; Trimethyl borate; oxygen; copper diacetate; palladium diacetate; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
2: |Suzuki-Miyaura Coupling;
DOI:10.1021/jm301268u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 20 °C
2: copper diacetate; pyridine; oxygen / dimethyl sulfoxide / 96 h / 40 - 50 °C
With
pyridine; N-Bromosuccinimide; oxygen; copper diacetate;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm301268u
