(1-(9-(1,3-dioxolan-2-yl)nonyl)piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate

Base Information

Chemical Name:(1-(9-(1,3-dioxolan-2-yl)nonyl)piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
CAS No.:1415971-16-2
Molecular Formula:C₃₂H₅₁NO₅
Molecular Weight:529.761
Hs Code.:

Synonyms:(1-(9-(1,3-dioxolan-2-yl)nonyl)piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate

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Chemical Property of (1-(9-(1,3-dioxolan-2-yl)nonyl)piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate

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Technology Process of (1-(9-(1,3-dioxolan-2-yl)nonyl)piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate

There total 6 articles about (1-(9-(1,3-dioxolan-2-yl)nonyl)piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59014-60-7
2-(9-bromononyl)-1,3-dioxacyclopentane

: 1415971-15-1
(piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate hydrochloride

: 1415971-16-2
(1-(9-(1,3-dioxolan-2-yl)nonyl)piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 60 ℃; for 17h;

Reference yield:

: 4335-77-7,20585-34-6,20585-39-1,50896-04-3
cyclohexylmandelic acid

: 1415971-16-2
(1-(9-(1,3-dioxolan-2-yl)nonyl)piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C

2: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 17 h / 60 °C

With hydrogenchloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1415971-14-0
tert-butyl 4-((2-cyclohexyl-2-hydroxy-2-phenylacetyloxy)methyl)piperidine-1-carboxylate

: 1415971-16-2
(1-(9-(1,3-dioxolan-2-yl)nonyl)piperidin-4-yl)methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 17 h / 60 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; acetonitrile;