methanesulfonic acid [5-(4-methoxy-2-trifluoromethylphenyl)-[1,3,4]thiadiazol-2-yl]methanyl ester

Base Information

Chemical Name:methanesulfonic acid [5-(4-methoxy-2-trifluoromethylphenyl)-[1,3,4]thiadiazol-2-yl]methanyl ester
CAS No.:1350351-94-8
Molecular Formula:C₁₂H₁₁F₃N₂O₄S₂
Molecular Weight:368.358
Hs Code.:

Synonyms:methanesulfonic acid [5-(4-methoxy-2-trifluoromethylphenyl)-[1,3,4]thiadiazol-2-yl]methanyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methanesulfonic acid [5-(4-methoxy-2-trifluoromethylphenyl)-[1,3,4]thiadiazol-2-yl]methanyl ester

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Technology Process of methanesulfonic acid [5-(4-methoxy-2-trifluoromethylphenyl)-[1,3,4]thiadiazol-2-yl]methanyl ester

There total 2 articles about methanesulfonic acid [5-(4-methoxy-2-trifluoromethylphenyl)-[1,3,4]thiadiazol-2-yl]methanyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1350351-93-7
[5-(4-methoxy-2-trifluoromethylphenyl)-[1,3,4]thiadiazol-2-yl]-methanol

: 7143-01-3
Methanesulfonic anhydride

: 1350351-94-8
methanesulfonic acid [5-(4-methoxy-2-trifluoromethylphenyl)-[1,3,4]thiadiazol-2-yl]methanyl ester

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1350351-92-6
2-(4-methoxy-2-trifluoromethylphenyl)-5-triisopropylsilanyloxymethyl-[1,3,4]thiadiazole

: 1350351-94-8
methanesulfonic acid [5-(4-methoxy-2-trifluoromethylphenyl)-[1,3,4]thiadiazol-2-yl]methanyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

2: pyridine / dichloromethane / 1 h / 20 °C

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;