1-phenylethyl trifluoroethanedithioate

Base Information

• Chemical Name: 1-phenylethyl trifluoroethanedithioate
• CAS No.: 1240463-52-8
• Molecular Formula: C₁₀H₉F₃S₂
• Molecular Weight: 250.309

Synonyms:1-phenylethyl trifluoroethanedithioate

Chemical Property of 1-phenylethyl trifluoroethanedithioate

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Technology Process of 1-phenylethyl trifluoroethanedithioate

There total 1 articles about 1-phenylethyl trifluoroethanedithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

trifluoro methylthiocarbonylchloride (2375-37-3) + 1-Phenylethanethiol (33877-11-1,33877-16-6,75081-57-1,6263-65-6) → 1-phenylethyl trifluoroethanedithioate (1240463-52-8)

Guidance literature:

In diethyl ether; hexane; at 20 ℃; for 16h;

DOI:10.1016/j.jfluchem.2009.11.011

Reference yield: 98.0%

1-phenylethyl trifluoroethanedithioate (1240463-52-8) + buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) → 2-[(1-phenylethyl)thio]-2-trifluoromethyl-3,6-dihydro-2H-thiopyran (1240463-67-5)

Guidance literature:

In benzene; at 20 ℃; for 24h; optical yield given as %de;

DOI:10.1016/j.jfluchem.2009.11.011

Reference yield: 94.0%

1-phenylethyl trifluoroethanedithioate (1240463-52-8) + 2,3-dimethyl-buta-1,3-diene (513-81-5) → 4,5-dimethyl-2-[(1-phenylethyl)thio]-2-trifluoromethyl-3,6-dihydro-2H-thiopyran (1240463-65-3)

Guidance literature:

at -20 ℃; for 16h; optical yield given as %de;

DOI:10.1016/j.jfluchem.2009.11.011

upstream raw materials:

trifluoro methylthiocarbonylchloride

1-Phenylethanethiol

Downstream raw materials:

3-[(1-phenylethyl)thio]-3-trifluoromethyl-2-thiabicyclo[2.2.1]hept-5-ene

2-[(1-phenylethyl)thio]-2-trifluoromethyl-3,6-dihydro-2H-thiopyran

4,5-dimethyl-2-[(1-phenylethyl)thio]-2-trifluoromethyl-3,6-dihydro-2H-thiopyran

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