5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline hydrochloride

Base Information

• Chemical Name: 5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline hydrochloride
• CAS No.: 957203-93-9
• Molecular Formula: C₂₀H₁₆F₃NOS*ClH
• Molecular Weight: 411.875

Synonyms:5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline hydrochloride

Chemical Property of 5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline hydrochloride

Chemical Property:

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Technology Process of 5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline hydrochloride

There total 1 articles about 5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-tert-butoxycarbonyl-5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline (957203-92-8) → 5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline hydrochloride (957203-93-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 14h;

Reference yield:

5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline hydrochloride (957203-93-9) + chloroacetyl chloride (79-04-9) → 1-(2-chloroacetyl)-5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline (957204-54-5)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

ethyl 6-(chloroformyl)hexanoate (14794-32-2) + 5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline hydrochloride (957203-93-9) → 7-oxo-7-[5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indolin-1-yl]heptanoic acid ethyl ester (957204-02-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;

upstream raw materials:

1-tert-butoxycarbonyl-5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline

Downstream raw materials:

3-[N-[2-oxo-2-[5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indolin-1-yl]ethyl]amino]propionic acid ethyl ester

1-[5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indolin-1-ylcarbonyl]azetidine-3-carboxylic acid methyl ester

4-[N-[5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indolin-1-ylcarbonyl]amino]butyric acid ethyl ester

1-(2-chloroacetyl)-5-[(4-phenyl-5-trifluoromethyl-2-thienyl)methoxy]indoline

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