(2S,3S)-2,3-bis[(4-methylbenzoyl)oxy]butanedioic acid 1-(R)-(cyclopropylsulphonimidoyl)-4-nitrobenzene

Base Information

Chemical Name:(2S,3S)-2,3-bis[(4-methylbenzoyl)oxy]butanedioic acid 1-(R)-(cyclopropylsulphonimidoyl)-4-nitrobenzene
CAS No.:1365544-29-1
Molecular Formula:C₉H₁₀N₂O₃S*C₂₀H₁₈O₈
Molecular Weight:612.614
Hs Code.:

Synonyms:(2S,3S)-2,3-bis[(4-methylbenzoyl)oxy]butanedioic acid 1-(R)-(cyclopropylsulphonimidoyl)-4-nitrobenzene

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Chemical Property of (2S,3S)-2,3-bis[(4-methylbenzoyl)oxy]butanedioic acid 1-(R)-(cyclopropylsulphonimidoyl)-4-nitrobenzene

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Technology Process of (2S,3S)-2,3-bis[(4-methylbenzoyl)oxy]butanedioic acid 1-(R)-(cyclopropylsulphonimidoyl)-4-nitrobenzene

There total 4 articles about (2S,3S)-2,3-bis[(4-methylbenzoyl)oxy]butanedioic acid 1-(R)-(cyclopropylsulphonimidoyl)-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.4%

: 942410-33-5
cyclopropyl(imino)(4-nitrophenyl)-λ⁶-sulfanone

: 32634-68-7
(2S,3S)-di-4-toluoyltartaric acid

: 1365544-29-1
(2S,3S)-2,3-bis[(4-methylbenzoyl)oxy]butanedioic acid 1-(R)-(cyclopropylsulphonimidoyl)-4-nitrobenzene

Guidance literature:: In acetonitrile; at 20 ℃; for 16h;

Reference yield:

: 1365543-59-4
N-[cyclopropyl(4-nitrophenyl)-lambda⁴-sulphanylidene]-2,2,2-trifluoroacetamide

: 1365544-29-1
(2S,3S)-2,3-bis[(4-methylbenzoyl)oxy]butanedioic acid 1-(R)-(cyclopropylsulphonimidoyl)-4-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; Oxone / methanol; sulfolane; water / 1 h / 25 °C / pH 10

2: acetonitrile / 16 h / 20 °C

With Oxone; potassium carbonate; In sulfolane; methanol; water; acetonitrile;

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 1365544-29-1
(2S,3S)-2,3-bis[(4-methylbenzoyl)oxy]butanedioic acid 1-(R)-(cyclopropylsulphonimidoyl)-4-nitrobenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 0.5 h / 30 °C

1.2: 8 h / 135 - 140 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 5 °C

2.2: 14.25 h / 20 - 25 °C

3.1: potassium carbonate; Oxone / methanol; sulfolane; water / 1 h / 25 °C / pH 10

4.1: acetonitrile / 16 h / 20 °C

With Oxone; sodium hydride; potassium carbonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; sulfolane; methanol; water; acetonitrile; mineral oil;