N-(3-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-3,3,3-trifluoro-propanamide

Base Information

Chemical Name:N-(3-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-3,3,3-trifluoro-propanamide
CAS No.:1071927-76-8
Molecular Formula:C₂₀H₁₄Cl₂F₆N₂O₂
Molecular Weight:499.24
Hs Code.:

Synonyms:N-(3-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-3,3,3-trifluoro-propanamide

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Chemical Property of N-(3-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-3,3,3-trifluoro-propanamide

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Technology Process of N-(3-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-3,3,3-trifluoro-propanamide

There total 6 articles about N-(3-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-3,3,3-trifluoro-propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: C₁₁H₁₀ClF₃N₂O₂

: 1071927-76-8
N-(3-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-3,3,3-trifluoro-propanamide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 15h;

Reference yield:

: 1071927-91-7
methyl 3-((3,3,3-trifluoropropionyl)amino)-2-methyl-benzoate

: 1071927-76-8
N-(3-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-3,3,3-trifluoro-propanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 0 °C

1.2: 0 °C

2.1: manganese(IV) oxide / chloroform / 14 h / 20 °C

3.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 0.33 h / 20 °C

4.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0.5 h / 50 °C

5.1: triethylamine / N,N-dimethyl-formamide / 15 h / 20 °C

With manganese(IV) oxide; N-chloro-succinimide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium acetate; triethylamine; In tetrahydrofuran; ethanol; chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: 1071927-74-6
N-(3,3,3-trifluoro-propionyl)-2-mehyl-3-hydroxyiminomethyl-aniline

: 1071927-76-8
N-(3-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-3,3,3-trifluoro-propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide / N,N-dimethyl-formamide / 0.5 h / 50 °C

2: triethylamine / N,N-dimethyl-formamide / 15 h / 20 °C

With N-chloro-succinimide; triethylamine; In N,N-dimethyl-formamide;