4-(2-hydroxy-ethoxy)-2,6-bis-methoxymethyl-4-methyl-cyclohexa-2,5-dienone

Base Information

Chemical Name:4-(2-hydroxy-ethoxy)-2,6-bis-methoxymethyl-4-methyl-cyclohexa-2,5-dienone
CAS No.:941282-88-8
Molecular Formula:C₁₃H₂₀O₅
Molecular Weight:256.299
Hs Code.:

Synonyms:4-(2-hydroxy-ethoxy)-2,6-bis-methoxymethyl-4-methyl-cyclohexa-2,5-dienone

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Chemical Property of 4-(2-hydroxy-ethoxy)-2,6-bis-methoxymethyl-4-methyl-cyclohexa-2,5-dienone

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Technology Process of 4-(2-hydroxy-ethoxy)-2,6-bis-methoxymethyl-4-methyl-cyclohexa-2,5-dienone

There total 4 articles about 4-(2-hydroxy-ethoxy)-2,6-bis-methoxymethyl-4-methyl-cyclohexa-2,5-dienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 32449-09-5
2,6-bis(methoxymethyl)-4-methylphenol

: 107-21-1
ethylene glycol

: 941282-88-8
4-(2-hydroxy-ethoxy)-2,6-bis-methoxymethyl-4-methyl-cyclohexa-2,5-dienone

Guidance literature:: With [bis(acetoxy)iodo]benzene; In dichloromethane; at 23 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/op600278f

Reference yield:

: 106-44-5
p-cresol

: 941282-88-8
4-(2-hydroxy-ethoxy)-2,6-bis-methoxymethyl-4-methyl-cyclohexa-2,5-dienone

Guidance literature:: Multi-step reaction with 4 steps

1: 39 percent / aq. NaOH / 12 h

2: 94 percent / HCl / 12 h

3: 78 percent / NaOMe / 12 h

4: PhI(OAc)2 / CH₂Cl₂ / 2.5 h / 20 °C

With hydrogenchloride; sodium hydroxide; [bis(acetoxy)iodo]benzene; sodium methylate; In dichloromethane;
DOI:10.1021/ja058337u

Reference yield:

: 91-04-3
2,6-bis(hydroxymethyl)-4-methylphenol

: 941282-88-8
4-(2-hydroxy-ethoxy)-2,6-bis-methoxymethyl-4-methyl-cyclohexa-2,5-dienone

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / HCl / 12 h

2: 78 percent / NaOMe / 12 h

3: PhI(OAc)2 / CH₂Cl₂ / 2.5 h / 20 °C

With hydrogenchloride; [bis(acetoxy)iodo]benzene; sodium methylate; In dichloromethane;
DOI:10.1021/ja058337u