Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine

Base Information

• Chemical Name: Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine
• CAS No.: 108607-50-7
• Molecular Formula: C₃₆H₃₇N₃O₇S
• Molecular Weight: 655.772
• Mol file: 108607-50-7.mol

Synonyms:Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine

Chemical Property of Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine

There total 6 articles about Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine methyl ester (108517-79-9) → Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine (108607-50-7)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; for 3h; Ambient temperature;

Reference yield: 62.0%

Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine phenylhydrazide (108607-49-4) → Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine (108607-50-7)

Guidance literature:

With iron(III) chloride; In 1,4-dioxane; water; at 35 ℃; for 0.5h;

Reference yield:

S-benzyl-N-[(benzyloxy)carbonyl]cysteinyltyrosine (39621-64-2) → Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine (108607-50-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / CaCl₂, thermolysin / dimethylformamide; various solvent(s) / 24 h / 38 °C / pH 7.0

2: 74 percent / 1 M NaOH / dioxane / 3 h / Ambient temperature

With sodium hydroxide; calcium chloride; thermolysin; In 1,4-dioxane; N,N-dimethyl-formamide;

upstream raw materials:

Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine methyl ester

Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanine phenylhydrazide

S-benzyl-N-[(benzyloxy)carbonyl]cysteinyltyrosine

benzyloxycarbonyl-S-benzylcysteinyl-tyrosine ethyl ester

Downstream raw materials:

Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine

pressinoic acid (disulfide)

Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-benzylcysteine phenylhydrazide

Refernces