(R)-4-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-4-hydroxy-N-methoxy-N-methylbutanamide

Base Information

Chemical Name:(R)-4-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-4-hydroxy-N-methoxy-N-methylbutanamide
CAS No.:1063713-72-3
Molecular Formula:C₁₉H₂₉NO₅
Molecular Weight:351.443
Hs Code.:

Synonyms:(R)-4-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-4-hydroxy-N-methoxy-N-methylbutanamide

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Chemical Property of (R)-4-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-4-hydroxy-N-methoxy-N-methylbutanamide

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Technology Process of (R)-4-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-4-hydroxy-N-methoxy-N-methylbutanamide

There total 1 articles about (R)-4-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-4-hydroxy-N-methoxy-N-methylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1063713-70-1
(R)-5-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-dihydrofuran-2(3H)-one

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1063713-72-3
(R)-4-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-4-hydroxy-N-methoxy-N-methylbutanamide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With tert-butylmagnesium chloride; In tetrahydrofuran; diethyl ether; at -8 ℃; for 0.166667h; Inert atmosphere;

(R)-5-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-dihydrofuran-2(3H)-one; In tetrahydrofuran; diethyl ether; at -10 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/ol801585j

Reference yield:

: 1063713-72-3
(R)-4-((2R,5R)-5-(benzyloxymethyl)-5-methyl-tetrahydrofuran-2-yl)-4-hydroxy-N-methoxy-N-methylbutanamide

: 1063713-85-8
C₁₉H₂₇NO₅

Guidance literature:: C₅₈H₆₉NO₁₇; With potassium hydroxide; In tetrahydrofuran; water; at 20 - 60 ℃;

With hydrogenchloride; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol801519j