4,10-bis(p-tolylsulphonyl)-7,16,21-trioxa-1,4,10,13-tetra-azabicyclo<11.5.5>tricosane

Base Information

Chemical Name:4,10-bis(p-tolylsulphonyl)-7,16,21-trioxa-1,4,10,13-tetra-azabicyclo<11.5.5>tricosane
CAS No.:118074-99-0
Molecular Formula:C₃₀H₄₆N₄O₇S₂
Molecular Weight:638.85
Hs Code.:

Synonyms:4,10-bis(p-tolylsulphonyl)-7,16,21-trioxa-1,4,10,13-tetra-azabicyclo<11.5.5>tricosane

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Chemical Property of 4,10-bis(p-tolylsulphonyl)-7,16,21-trioxa-1,4,10,13-tetra-azabicyclo<11.5.5>tricosane

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Technology Process of 4,10-bis(p-tolylsulphonyl)-7,16,21-trioxa-1,4,10,13-tetra-azabicyclo<11.5.5>tricosane

There total 4 articles about 4,10-bis(p-tolylsulphonyl)-7,16,21-trioxa-1,4,10,13-tetra-azabicyclo<11.5.5>tricosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 5414-19-7
1,1'-oxybis(2-bromo-ethane)

: 118074-98-9
4,10-bis<2-(p-tolylsulphonylamino)ethyl>-1,7-dioxa-4,10-diazacyclododecane

: 118074-99-0
4,10-bis(p-tolylsulphonyl)-7,16,21-trioxa-1,4,10,13-tetra-azabicyclo<11.5.5>tricosane

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In toluene; for 16h; Heating;

Reference yield: 81.0%

: 118074-98-9
4,10-bis<2-(p-tolylsulphonylamino)ethyl>-1,7-dioxa-4,10-diazacyclododecane

: 7460-82-4
diethylene glycol ditosylate

: 118074-99-0
4,10-bis(p-tolylsulphonyl)-7,16,21-trioxa-1,4,10,13-tetra-azabicyclo<11.5.5>tricosane

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In toluene;

Reference yield:

: 294-92-8
diaza[12]crown-4

: 118074-99-0
4,10-bis(p-tolylsulphonyl)-7,16,21-trioxa-1,4,10,13-tetra-azabicyclo<11.5.5>tricosane

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / acetonitrile / Heating

2: 81 percent / 45percent aq. NaOH, tetrabutylammonium iodide / toluene

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In toluene; acetonitrile;