N'-hydroxy-4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzene-carboximidamide hydroformiate

Base Information

Chemical Name:N'-hydroxy-4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzene-carboximidamide hydroformiate
CAS No.:1085453-56-0
Molecular Formula:CH₂O₂*C₁₂H₁₆N₂O₃
Molecular Weight:282.296
Hs Code.:

Synonyms:N'-hydroxy-4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzene-carboximidamide hydroformiate

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Chemical Property of N'-hydroxy-4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzene-carboximidamide hydroformiate

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Technology Process of N'-hydroxy-4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzene-carboximidamide hydroformiate

There total 4 articles about N'-hydroxy-4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzene-carboximidamide hydroformiate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 64-18-6
formic acid

: 1085453-54-8
4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzenecarbonitrile

: 1085453-56-0
N'-hydroxy-4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzene-carboximidamide hydroformiate

Guidance literature:: 4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzenecarbonitrile; With hydroxylamine hydrochloride; triethylamine; In ethanol; for 4h; Heating / reflux;

formic acid; at 20 ℃;

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 1085453-56-0
N'-hydroxy-4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzene-carboximidamide hydroformiate

Guidance literature:: Multi-step reaction with 2 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran; diethyl ether / 1.5 h / -40 °C

1.2: 2.67 h / -78 - 20 °C

2.1: hydroxylamine hydrochloride; triethylamine / ethanol / 4 h / Heating / reflux

2.2: 20 °C

With hydroxylamine hydrochloride; isopropylmagnesium chloride; triethylamine; In tetrahydrofuran; diethyl ether; ethanol;

Reference yield:

: 3058-39-7
4-iodobenzonitrile

: 1085453-56-0
N'-hydroxy-4-(4-hydroxytetrahydro-2H-pyran-4-yl)benzene-carboximidamide hydroformiate

Guidance literature:: Multi-step reaction with 2 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran; diethyl ether / 1.5 h / -40 °C

1.2: 2.67 h / -78 - 20 °C

2.1: hydroxylamine hydrochloride; triethylamine / ethanol / 4 h / Heating / reflux

2.2: 20 °C

With hydroxylamine hydrochloride; isopropylmagnesium chloride; triethylamine; In tetrahydrofuran; diethyl ether; ethanol;