tri-O-benzyl-2-deoxy-1-O-methoxyacetylglucose

Base Information

Chemical Name:tri-O-benzyl-2-deoxy-1-O-methoxyacetylglucose
CAS No.:256390-79-1
Molecular Formula:C₃₀H₃₄O₇
Molecular Weight:506.596
Hs Code.:

Synonyms:tri-O-benzyl-2-deoxy-1-O-methoxyacetylglucose

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Chemical Property of tri-O-benzyl-2-deoxy-1-O-methoxyacetylglucose

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Technology Process of tri-O-benzyl-2-deoxy-1-O-methoxyacetylglucose

There total 2 articles about tri-O-benzyl-2-deoxy-1-O-methoxyacetylglucose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 160549-11-1
3,4,6-tri-O-benzyl-2-deoxy-D-glucopyranose

: 625-45-6
2-methoxyacetic acid

: 256390-79-1
tri-O-benzyl-2-deoxy-1-O-methoxyacetylglucose

Guidance literature:: 3,4,6-tri-O-benzyl-2-deoxy-D-glucopyranose; With dicyclohexyl-carbodiimide; In diethyl ether; at 20 ℃; for 0.166667h;

2-methoxyacetic acid; With 4-pyrrolidin-1-ylpyridine; In diethyl ether;
DOI:10.1139/v02-095

Reference yield:

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 256390-79-1
tri-O-benzyl-2-deoxy-1-O-methoxyacetylglucose

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphonium bromide / tetrahydrofuran / 0.17 h / 20 °C

1.2: 81 percent / water / tetrahydrofuran / 3 h / 20 °C

2.1: dicyclohexylcarbodiimide / diethyl ether / 0.17 h / 20 °C

2.2: 87 percent / 4-pyrrolidinopyridine / diethyl ether

With triphenylphosphine hydrobromide; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether;
DOI:10.1139/v02-095