(S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline

Base Information

Chemical Name:(S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline
CAS No.:640736-36-3
Molecular Formula:C₂₅H₃₃NO
Molecular Weight:363.543
Hs Code.:

Synonyms:(S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline

Chemical Property:

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Technology Process of (S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline

There total 1 articles about (S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 255850-24-9
4-acetylenyl-2,6-dimethylaniline

: 5-Iodo-1,3-dimethyl-2-((S)-1-methyl-hexyloxy)-benzene

: 640736-36-3
(S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 50 - 70 ℃; for 24h;
DOI:10.1016/S0022-328X(03)00763-0

Reference yield: 96.0%

: 64-18-6
formic acid

: 640736-36-3
(S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline

: 640736-48-7
(S)-4-(4-(1-methylhexyloxy-2,6-dimethyl)phenylethynyl)-2,6-dimethyl-1-formamidobenzene

Guidance literature:: formic acid; With acetic anhydride; at 50 - 60 ℃; for 2h;

(S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline; at 20 ℃; for 24h;
DOI:10.1016/S0022-328X(03)00763-0

Reference yield:

: 640736-36-3
(S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylaniline

: 640736-60-3
(S)-4-(4-(1-methylhexyloxy)-2,6-dimethylphenylethynyl)-2,6-dimethylphenylisocyanide

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydrie / 2 h / 50 - 60 °C

1.2: 96 percent / 24 h / 20 °C

2.1: 80 percent / triethylamine; triphosgene / CH₂Cl₂ / 12 h / 20 °C

With bis(trichloromethyl) carbonate; acetic anhydride; triethylamine; In dichloromethane;
DOI:10.1016/S0022-328X(03)00763-0