4-acetylbenzenesulfonyl azide

Base Information

Chemical Name:4-acetylbenzenesulfonyl azide
CAS No.:75177-14-9
Molecular Formula:C₈H₇N₃O₃S
Molecular Weight:225.228
Hs Code.:

Synonyms:4-acetylbenzenesulfonyl azide

Suppliers and Price of 4-acetylbenzenesulfonyl azide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetylbenzenesulfonyl azide

Chemical Property:

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Technology Process of 4-acetylbenzenesulfonyl azide

There total 3 articles about 4-acetylbenzenesulfonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 455-25-4
4-acetylbenzene-1-sulfonyl fluoride

: 75177-14-9
4-acetylbenzenesulfonyl azide

Guidance literature:: With trimethylsilylazide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1055/s-0035-1561626

Reference yield: 76.0%

: 1565-17-9
4-acetylbenzenesulfonamide

: 75177-14-9
4-acetylbenzenesulfonyl azide

Guidance literature:: With 3-azidosulfonyl-3H-imidazole-1-ium hydrogen sulfate; potassium carbonate; In water; isopropyl alcohol; at 20 ℃; for 18h;
DOI:10.1021/jo500553q

Reference yield:

: 455-20-9
4-ethylbenzenesulfonyl fluoride

: 75177-14-9
4-acetylbenzenesulfonyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: KMnO₄; Mg(NO₃)2; aqueous acetone

2: NaN₃

With magnesium(II) nitrate; potassium permanganate; sodium azide; acetone;