(E)-5-[Benzyl-(2-cyano-ethyl)-amino]-pent-3-enoic acid ethyl ester

Base Information

• Chemical Name: (E)-5-[Benzyl-(2-cyano-ethyl)-amino]-pent-3-enoic acid ethyl ester
• CAS No.: 119804-11-4
• Molecular Formula: C₁₇H₂₂N₂O₂
• Molecular Weight: 286.374
• Mol file: 119804-11-4.mol

Synonyms:(E)-5-[Benzyl-(2-cyano-ethyl)-amino]-pent-3-enoic acid ethyl ester

Chemical Property of (E)-5-[Benzyl-(2-cyano-ethyl)-amino]-pent-3-enoic acid ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (E)-5-[Benzyl-(2-cyano-ethyl)-amino]-pent-3-enoic acid ethyl ester

There total 1 articles about (E)-5-[Benzyl-(2-cyano-ethyl)-amino]-pent-3-enoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

ethanol (64-17-5) + carbon monoxide (201230-82-2) + Acetic acid (E)-4-[benzyl-(2-cyano-ethyl)-amino]-but-2-enyl ester (119804-09-0) → (E)-5-[Benzyl-(2-cyano-ethyl)-amino]-pent-3-enoic acid ethyl ester (119804-11-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenylphosphine; sodium bromide; at 50 ℃; for 20h; under 22065.2 Torr; further reagents and further catalysts;

DOI:10.1016/S0040-4039(00)80648-6

upstream raw materials:

ethanol

carbon monoxide

Acetic acid (E)-4-[benzyl-(2-cyano-ethyl)-amino]-but-2-enyl ester