5-[4-(3-methyl-5-phenylsulfanyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

Base Information

Chemical Name:5-[4-(3-methyl-5-phenylsulfanyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione
CAS No.:172648-63-4
Molecular Formula:C₄₃H₃₄N₄O₃S₂
Molecular Weight:718.9
Hs Code.:

Synonyms:5-[4-(3-methyl-5-phenylsulfanyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

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Chemical Property of 5-[4-(3-methyl-5-phenylsulfanyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

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Technology Process of 5-[4-(3-methyl-5-phenylsulfanyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

There total 7 articles about 5-[4-(3-methyl-5-phenylsulfanyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10465-81-3,871024-86-1
1,1'-(Azodicarbonyl)dipiperidin

: 150556-72-2
5-(4-hydroxy-benzyl)-3-triphenylmethylthiazolidine-2,4-dione

: 5-[4-(1-t-Butoxycarbonylindolin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazoliine-2,4-dione

: 172648-63-4
5-[4-(3-methyl-5-phenylsulfanyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

Guidance literature:: With tributylphosphine; In toluene;

Reference yield:

: 16013-85-7,136901-10-5
2,6-dicholoro-3-nitropyridine

: 172648-63-4
5-[4-(3-methyl-5-phenylsulfanyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / Na₂CO₃ / ethanol / 8 h / 20 °C

2: methanol / 3 h / 20 °C

3: H₂ / 10percent Pd/C / dioxane / 5 h / 80 °C

4: toluene / 4 h / Heating

5: azodicarbonyldipieridine; Bu₃P / toluene / 4 h / 20 °C

With tributylphosphine; hydrogen; sodium carbonate; 1,1'-azodicarbonyl-dipiperidine; 10percent Pd/C; In 1,4-dioxane; methanol; ethanol; toluene; 1: Amination / 2: Akoxylation / 3: Catalytic hydrogenation / 4: Cyclization / 5: Mitsunobu reaction;
DOI:10.1021/jm990522t

Reference yield:

: 930-69-8
sodium thiophenolate

: 172648-63-4
5-[4-(3-methyl-5-phenylsulfanyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / 3 h / 20 °C

2: H₂ / 10percent Pd/C / dioxane / 5 h / 80 °C

3: toluene / 4 h / Heating

4: azodicarbonyldipieridine; Bu₃P / toluene / 4 h / 20 °C

With tributylphosphine; hydrogen; 1,1'-azodicarbonyl-dipiperidine; 10percent Pd/C; In 1,4-dioxane; methanol; toluene; 1: Akoxylation / 2: Catalytic hydrogenation / 3: Cyclization / 4: Mitsunobu reaction;
DOI:10.1021/jm990522t