1-(4-methoxybenzyl)-2-methylideneaziridine

Base Information

Chemical Name:1-(4-methoxybenzyl)-2-methylideneaziridine
CAS No.:1070895-95-2
Molecular Formula:C₁₁H₁₃NO
Molecular Weight:175.23
Hs Code.:

Synonyms:1-(4-methoxybenzyl)-2-methylideneaziridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-methoxybenzyl)-2-methylideneaziridine

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Technology Process of 1-(4-methoxybenzyl)-2-methylideneaziridine

There total 2 articles about 1-(4-methoxybenzyl)-2-methylideneaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 96850-73-6
(2-bromoallyl)-(4-methoxybenzyl)-amine

: 1070895-95-2
1-(4-methoxybenzyl)-2-methylideneaziridine

Guidance literature:: With Iron(III) nitrate nonahydrate; ammonia; sodium amide; In diethyl ether; at -33 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo801664g

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 1070895-95-2
1-(4-methoxybenzyl)-2-methylideneaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

2: ammonia; sodium amide / diethyl ether / 1 h / -78 °C

With ammonia; potassium carbonate; sodium amide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/c3cc41061g

Reference yield: 81.0%

: 31699-35-1
2,7-nonadiyne

: 1070895-95-2
1-(4-methoxybenzyl)-2-methylideneaziridine

: 1437300-31-6
4-(hex-4-yn-1-yl)-1-(4-methoxybenzyl)-2,3-dimethyl-1H-pyrrole

Guidance literature:: With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; In 1,4-dioxane; at 20 ℃; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3cc41061g