(Z)-2-(2-bromo-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-2-(2-bromo-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1361146-99-7
Molecular Formula:C₁₄H₂₄BBrO₂
Molecular Weight:315.058
Hs Code.:

Synonyms:(Z)-2-(2-bromo-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(2-bromo-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (Z)-2-(2-bromo-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 2 articles about (Z)-2-(2-bromo-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 931-48-6
2-cyclohexylacetylene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1361146-99-7
(Z)-2-(2-bromo-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 2-cyclohexylacetylene; With boron tribromide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; Inert atmosphere;
DOI:10.1002/anie.201105716

Reference yield: 35.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 931-48-6
2-cyclohexylacetylene

: 10294-33-4
boron tribromide

: 1361146-99-7
(Z)-2-(2-bromo-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 2-cyclohexylacetylene; boron tribromide; In dichloromethane; at -78 - 20 ℃; for 2h;

2,3-dimethyl-2,3-butane diol; In dichloromethane; at -78 - 20 ℃; for 2h;

Reference yield: 90.0%

: 1361146-99-7
(Z)-2-(2-bromo-2-cyclohexylvinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 676-58-4
methylmagnesium chloride

: 1361147-00-3
(E)-2-(2-cyclohexylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; zinc dibromide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/anie.201105716