5-(5-methyl-1-phenyl-1H-4-pyrazolyl)-1,3,4-oxadiazol-2-yl hydrosulfide

Base Information

Chemical Name:5-(5-methyl-1-phenyl-1H-4-pyrazolyl)-1,3,4-oxadiazol-2-yl hydrosulfide
CAS No.:816429-52-4
Molecular Formula:C₁₂H₁₀N₄OS
Molecular Weight:258.304
Hs Code.:

Synonyms:5-(5-methyl-1-phenyl-1H-4-pyrazolyl)-1,3,4-oxadiazol-2-yl hydrosulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(5-methyl-1-phenyl-1H-4-pyrazolyl)-1,3,4-oxadiazol-2-yl hydrosulfide

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Technology Process of 5-(5-methyl-1-phenyl-1H-4-pyrazolyl)-1,3,4-oxadiazol-2-yl hydrosulfide

There total 5 articles about 5-(5-methyl-1-phenyl-1H-4-pyrazolyl)-1,3,4-oxadiazol-2-yl hydrosulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 75-15-0,12122-00-8
carbon disulfide

: 204260-39-9
5-methyl-1-phenyl-1H-4-pyrazolecarbohydrazide

: 816429-52-4
5-(5-methyl-1-phenyl-1H-4-pyrazolyl)-1,3,4-oxadiazol-2-yl hydrosulfide

Guidance literature:: With potassium hydroxide; In ethanol; for 12h; Reflux;

Reference yield: 70.0%

: 204260-39-9
5-methyl-1-phenyl-1H-4-pyrazolecarbohydrazide

: 816429-52-4
5-(5-methyl-1-phenyl-1H-4-pyrazolyl)-1,3,4-oxadiazol-2-yl hydrosulfide

Guidance literature:: With carbon disulfide; potassium hydroxide; In ethanol; for 12h; Reflux;
DOI:10.1248/cpb.58.1328

Reference yield:

: 203186-58-7
(E)-ethyl 2-((dimethylamino)methylene)-3-oxobutanoate

: 816429-52-4
5-(5-methyl-1-phenyl-1H-4-pyrazolyl)-1,3,4-oxadiazol-2-yl hydrosulfide

Guidance literature:: Multi-step reaction with 3 steps

1: Reflux

2: ethanol / Reflux

3: potassium hydroxide / ethanol / Reflux

With potassium hydroxide; In ethanol;
DOI:10.1002/jhet.913