1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester

Base Information

Chemical Name:1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester
CAS No.:131550-40-8
Molecular Formula:C₂₅H₃₃NO₇
Molecular Weight:459.54
Hs Code.:

Synonyms:1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester

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Chemical Property of 1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester

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Technology Process of 1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester

There total 2 articles about 1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 628-21-7
1,4-Diiodobutane

: 131550-37-3
(S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester

: 131550-40-8
1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 18h;
DOI:10.1016/S0040-4039(00)97050-3

Reference yield:

: 30925-18-9
2-tert-butoxycarbonylamino-succinic acid 1-benzyl ester

: 131550-40-8
1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / (Im)2CO / acetonitrile / 25 °C

2: 55 percent / Na₂CO₃ / dimethylformamide / 18 h / 60 °C

With sodium carbonate; 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(00)97050-3

Reference yield: 71.0%

: 131550-40-8
1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester

: 131550-47-5
(S)-2-tert-Butoxycarbonylamino-4-cyclopentyl-4-oxo-butyric acid benzyl ester

Guidance literature:: With pyrrolidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In acetonitrile; at 25 ℃; for 18h;
DOI:10.1016/S0040-4039(00)97050-3